11/12/17
Probe: 3.2mm HX probe
Sample3: activated MMM_Beta_3#_13C2H4_275C_20min (from 4 mm rotor "4010"), 20mM TEKPol in TCE, wetness impregnation
12.5 kHz MAS, BP = 2230 mB, DP =2060mB
TSample = 92K, flow = 2000 l/h, TBearing = 108K, TDrive =95 K
13C CP
sr = -4220 Hz, ref to CH of adamantane at 29.45 ppm
1H pulse 2.6 us at 70 W, corresponding to 2.5 us, 100 kHz at 76 W
13C rf 3.6 us at 100 W
13 C CP 62 kHz (80 W) matched to  90kHz proton ( 62W)
1H pulse and decoupling  100kHz, Spinal64 Dec (76W)
T1 =  4.5 s (one component)
T1 =  13.0 s (two components)
d1 = 4.5 s * 1.3 = 6 s
MW Off
ns = 64